Geopolymers
Inorganic polymeric new materials
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Abdellah Bahmani
Abdellah Bahmani
Laboratoire de Physico-Chimie des Matériaux-Catalyse et Environnement, Faculté des Sciences, Département de Chimie, Université des Sciences et de la Technologie d’Oran, B.P. 1505, El-Mnaouer, 31000, Oran, Algeria
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Mayouf Sellami
Mayouf Sellami
Laboratoire de Physico-Chimie des Matériaux-Catalyse et Environnement, Faculté des Sciences, Département de Chimie, Université des Sciences et de la Technologie d’Oran, B.P. 1505, El-Mnaouer, 31000, Oran, Algeria
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Noureddine Bettahar
Noureddine Bettahar
Laboratoire de Physico-Chimie des Matériaux-Catalyse et Environnement, Faculté des Sciences, Département de Chimie, Université des Sciences et de la Technologie d’Oran, B.P. 1505, El-Mnaouer, 31000, Oran, Algeria
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Abstract
Bismuth mixed oxide powders were prepared by oxalate coprecipitation process. The thermal decomposition behaviour of the coprecipitate precursors has been followed by thermal analysis (TG-DTA) and FTIR spectroscopy. During the decomposition of the precursor, several intermediates species were detected and a mechanism of formation of mixed oxide by this method is proposed. After the thermal treatment, the precursor obtained of suggested formula Ca3[Bi6O6(C2O4)4(OH)3NO3]0.5H2O, has led to the formation of CaBi2O4 at shorter reaction time than the traditional ceramic method. In order to consolidate the results, the coprecipitation in absence of oxalic precipitant under the same conditions was examined. XRD and scanning electron spectroscopy were used to study particles sizes and morphology.
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
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Temperature dependence of the rate of reaction in thermal analysis
The Arrhenius equation in condensed phase kinetics
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