Geopolymers
Inorganic polymeric new materials
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R. Janík
R. Janík
Department of Chemical Technologies and Environment, University of Trenčín, 020 32, Púchov, Slovakia
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E. Jóna
E. Jóna
Department of Chemical Technologies and Environment, University of Trenčín, 020 32, Púchov, Slovakia
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M. Pajtášová
M. Pajtášová
Department of Chemical Technologies and Environment, University of Trenčín, 020 32, Púchov, Slovakia
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D. Ondrušová
D. Ondrušová
Department of Chemical Technologies and Environment, University of Trenčín, 020 32, Púchov, Slovakia
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P. Lizák
P. Lizák
Department of Industrial Design, Faculty of Industrial Technologies, Trenčín University of A. Dubček, Trenčín, Slovakia
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V. Pavlík
V. Pavlík
Department of Chemistry, University of Guelph, Guelph, ON, Canada
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R. Durný
R. Durný
Slovak Institute of Metrology, Karloveská 63, Bratislava, Slovakia
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S. C. Mojumdar
S. C. Mojumdar
Department of Chemical Technologies and Environment, University of Trenčín, 020 32, Púchov, Slovakia
Department of Chemistry, University of Guelph, Guelph, ON, Canada
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Department of Chemistry, University of Guelph, Guelph, ON, Canada
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Abstract
The influence of the 2-, 3-, and 4-OH phenols on the type of interaction with Co-exchanged montmorillonite and thermal properties of these materials were studied. The results of XRD, IR, and thermal (TG, DTG) analysis show that organic species are intercalated into the interlayer space of montmorillonite. Thermal decomposition in the temperature interval 20–700 °C of studied samples with 2- and 3-hydroxyphenol proceeds in three steps (the release of adsorbed H2O molecules, combustion/desorption of protonated hydroxy phenols and dehydroxylation), while the sample with 4-hydroxyphenol decompose in four steps (the new peak at ~222 °C corresponds to directly coordinated organic species). The effect of different position of the hydroxyl groups on the phenol ring on the thermal decomposition is evident.
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2. Šnircová, S, Jóna, E, Lajdová, Ľ, Jorík, V, Drábik, M, Pajtášová, M, Ondrušová, D, Mojumdar, SC 2009 Ni-exchanged montmorillonite with methyl-, dimethyl- and trimethylamine and their thermal properties. J Therm Anal Calorim 96 1 63–66 .
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8. Jóna, E, Rudinská, G, Sapietová, M, Pavlík, V, Drábik, M, Mojumdar, SC 2007 Interactions of heterocyclic compounds with monoionic forms of montmorillonite thermal IR–spectral and X-ray studies of Ni(II)-montmorillonite with 3-R-and 2-R pyridines (R = CH3, Cl, NH3). J Therm Anal Calorim 90 3 687–691 .
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9. Jóna, E, Kubranová, M, Sirota, A, Kopcová, M 2001 Thermal and infrared study of desorption of pyridine and pyridine derivatives from Ni-exchanged montmorillonite. J Therm Anal Calorim 63 3 807–813 .
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10. Mojumdar, SC, Raki, L 2006 Preparation, thermal, spectral and microscopic studies of calcium silicate hydrate-poly(acrylic acid) nanocomposite materials. J Therm Anal Calorim 85:99–105 .
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11. Sawant, SY, Verenkar, VMS, Mojumdar, SC 2007 Preparation, thermal, XRD, chemical and FT-IR spectral analysis of NiMn2O4 nanoparticles and respective precursor. J Therm Anal Calorim 90:669–672 .
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12. Porob, RA, Khan, SZ, Mojumdar, SC, Verenkar, VMS 2006 Synthesis TG, SDC and infrared spectral study of NiMn2(C4H4O4)3·6N2H4: a precursor for NiMn2O4 nanoparticles. J Therm Anal Calorim 86:605–608 .
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13. Mojumdar, SC, Varshney, KG, Agrawal, A 2006 Hybrid fibrous ion exchange materials: past, present and future. Res J Chem Environ 10:89–103.
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14. Doval, M, Palou, M, Mojumdar, SC 2006 Hydration behaviour of C2S and C2AS nanomaterials, synthesized by sol–gel method. J Therm Anal Calorim 86:595–599 .
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15. Mojumdar, SC, Moresoli, C, Simon, LC, Legge, RL 2011 Edible wheat gluten (WG) protein films: preparation, thermal, mechanical and spectral properties. J Therm Anal Calorim 104:929–936 .
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16. Varshney, G, Agrawal, A, Mojumdar, SC 2007 Pyridine based cerium(IV) phosphate hybrid fibrous ion exchanger: synthesis, characterization and thermal behaviour. J Therm Anal Calorim 90:731–734 .
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17. Mojumdar, SC, Melnik, M, Jona, E 2000 Thermal and spectral properties of Mg(II) and Cu(II) complexes with heterocyclic N-donor ligands. J Anal Appl Pyrolysis 53:149–160 .
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20. Meenakshisundarm, SP, Parthiban, S, Madhurambal, G, Mojumdar, SC 2008 Effect of chelating agent (1,10-phenanthroline) on potassium hydrogen phthalate crystals. J Therm Anal Calorim 94:21–25 .
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21. Rejitha, KS, Mathew, S 2010 Investigations on the thermal behavior of hexaamminenickel(II) sulphate using TG-MS and TR-XRD. Glob J Anal Chem 1 1 100–108.
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22. Pajtášová, M, Ondrušová, D, Jóna, E, Mojumdar, SC, Ľalíková, S, Bazyláková, T, Gregor, M 2010 Spectral and thermal characteristics of copper(II) carboxylates with fatty acid chains and their benzothiazole adducts. J Therm Anal Calorim 100:769–777 .
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23. Madhurambal, G, Ramasamy, P, Anbusrinivasan, P, Vasudevan, G, Kavitha, S, Mojumdar, SC 2008 Growth and characterization studies of 2-bromo-4′-chloro-acetophenone (BCAP) crystals. J Therm Anal Calorim 94:59–62 .
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24. Gonsalves, LR, Mojumdar, SC, Verenkar, VMS 2011 Synthesis and characterisation of Co0.8Zn0.2Fe2O4 nanoparticles. J Therm Anal Calorim 104:869–873 .
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25. Raileanu, M, Todan, L, Crisan, M, Braileanu, A, Rusu, A, Bradu, C, Carpov, A, Zaharescu, M 2010 Sol–gel materials with pesticide deliveryproperties. J Environ Protect 1:302–313 .
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26. Varshney, KG, Agrawal, A, Mojumdar, SC 2005 Pectin based cerium(IV) and thorium(IV) phosphates as novel hybrid fibrous ion exchangers synthesis, characterization and thermal behaviour. J Therm Anal Calorim 81:183–189 .
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27. Mojumdar, SC, Šimon, P, Krutošíková, A 2009 [1]Benzofuro[3,2-c]pyridine: synthesis and coordination reactions. J Therm Anal Calorim 96:103–109 .
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28. Moricová, K, Jóna, E, Plško, A, Mojumdar, SC 2010 Thermal stability of Li2O–SiO2–TiO2 gels evaluated by the induction period of crystallization. J Therm Anal Calorim 100:817–820 .
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29. Mojumdar, SC, Miklovic, J, Krutosikova, A, Valigura, D, Stewart, JM 2005 Furopyridines and furopyridine–Ni(II) complexes: synthesis, thermal and spectral characterization. J Therm Anal Calorim 81:211–215 .
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30. Vasudevan, G, AnbuSrinivasan, P, Madhurambal, G, Mojumdar, SC 2009 Thermal analysis, effect of dopants, spectral characterisation and growth aspects of KAP crystals. J Therm Anal Calorim 96:99–102 .
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1969 |
| Volumes per Year |
1 |
| Issues per Year |
24 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 1388-6150 (Print) |
| ISSN | 1588-2926 (Online) |
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Temperature dependence of the rate of reaction in thermal analysis
The Arrhenius equation in condensed phase kinetics
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