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  • 1 Sensors and Composites Group, School of Metallurgy and Materials, University of Birmingham, Edgbaston, Birmingham B15 2TT, UK
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Abstract

The authors have previously reported on an optical technique to enable the simultaneous and non-contact acquisition of spectral, thermal and physical information of a sample in a differential scanning calorimeter (DSC). This was achieved using a simple bifurcated fibre optic probe to link the DSC to a conventional Fourier transform infrared spectrometer and an optical spectrum analyser. The fibre optic probe was located over the sample and reference compartments of the DSC. In the current study, a series of experiments were designed to investigate the stability of DSC pans during heating from ambient to 230 °C. During the first heating cycle, the base of the aluminium pans used in these experiments was found to deform in a non-linear manner. The deformation characteristics of pans manufactured from copper and steel were also investigated. Annealing the aluminium pans was found to improve significantly the deformation or expansion characteristics.

  • 1. Dumitresu O , Crosby PA, Fernando GF. Thermal and spectral analysis of an epoxy/amine resin system. Presented at Cea de-a XI-A Conferinta Internationala, de Chimie si Inginerie, Chemica, Romania, 30 Sept-2 Oct. 1999.

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  • 2. Dumitrescu OR , Doyle C, and Fernando GF. Extending differential scanning calorimetry to include non-contact vibrational spectroscopy. 30th annual conference, North American thermal analysis society, 23–25 Sept 2002.

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  • 3. Degamber, B, Winter, D, Tetlow, J, Teagle, M, Fernando, GF 2004 Simultaneous DSC/FTIRS/TMA. J Meas Sci Technol 15 9 L5L10 .

  • 4. Degamber, B, Fernando, GF 2006 Fibre optic dilato-spectroscopic sensor: simultaneous thermal, spectral and physical analyses of materials. J Smart Mater Struct 15:10541058 .

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  • 5. JF Shackelford W Alexander eds. 2000 CRC materials science and engineering handbook 3 CRC Press New York.

Manuscript Submission: HERE

  • Impact Factor (2019): 2.731
  • Scimago Journal Rank (2019): 0.415
  • SJR Hirsch-Index (2019): 87
  • SJR Quartile Score (2019): Q3 Condensed Matter Physics
  • SJR Quartile Score (2019): Q3 Physical and Theoretical Chemistry
  • Impact Factor (2018): 2.471
  • Scimago Journal Rank (2018): 0.634
  • SJR Hirsch-Index (2018): 78
  • SJR Quartile Score (2018): Q2 Condensed Matter Physics
  • SJR Quartile Score (2018): Q2 Physical and Theoretical Chemistry

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
4
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)