Geopolymers
Inorganic polymeric new materials
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Muhammad Bisyrul Hafi Othman
Muhammad Bisyrul Hafi Othman
School of Material and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, Seri Ampangan, 14300, Nibong Tebal, Pulau Pinang, Malaysia
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Rafiza Ramli
Rafiza Ramli
School of Material and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, Seri Ampangan, 14300, Nibong Tebal, Pulau Pinang, Malaysia
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Zulkifli Mohamad Ariff
Zulkifli Mohamad Ariff
School of Material and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, Seri Ampangan, 14300, Nibong Tebal, Pulau Pinang, Malaysia
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Hazizan Md Akil
Hazizan Md Akil
School of Material and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, Seri Ampangan, 14300, Nibong Tebal, Pulau Pinang, Malaysia
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Zulkifli Ahmad
Zulkifli Ahmad
School of Material and Mineral Resources Engineering, Engineering Campus, Universiti Sains Malaysia, Seri Ampangan, 14300, Nibong Tebal, Pulau Pinang, Malaysia
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Abstract
The influence of the structure properties relationships of silicone incorporated polyimide (PI) on thermal stability was investigated by using single scan thermogravimetric analysis (TG) and differential scanning calorimetry (DSC) in nitrogen. Four systems have been synthesized based on monomer 4-(4-(1-(4-(4-aminophenoxy) phenyl)-1-methylethyl) phenoxy) aniline (BAPP)/3,3′,4,4′-Biphenyltetracarboxylic dianhydride including parent PI (S-1), PI siloxane copolymer (S-2 and S-3), and PI siloxane hybrid (S-4). The derivative thermogravimetric analysis (DTG) and DSC curves indicate a double and single stage decomposition process and glass transition temperature (Tg), respectively. While the PI, PIS, and PSH showed distinctive features towards thermal analysis, it was found that the rate of degradation (δα/δt) was influenced by the flexibility of Si–O–Si in the backbone and in Si–O–Si itself. These results revealed that the presence of Si–O–Si in either the backbone or matrix indicates its stability with regard to high thermal service applications.
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1969 |
| Volumes per Year |
1 |
| Issues per Year |
24 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 1388-6150 (Print) |
| ISSN | 1588-2926 (Online) |
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Temperature dependence of the rate of reaction in thermal analysis
The Arrhenius equation in condensed phase kinetics
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