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  • 1 CSGI, Unità Operativa di Pavia, Dipartimento di Chimica (Sezione di Chimica Fisica) della, Università di Pavia, Via Taramelli 16, 27100, Pavia, Italy
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Abstract

Simultaneous TG–DSC measurements have been used to study the solid state reaction in the system SnC2O4–4MgCO3·Mg(OH)2·xH2O (Sn:Mg = 0.5). The results obtained with physically prepared mixture and with mixture mechanically activated by high-energy milling are compared. Synthesis of the compound Mg2SnO4 has been attempted starting from both type of mixture: Mg2SnO4 forms by annealing the activated mixture at temperatures between 850 and 1,000 °C while it can hardly be obtained from physical mixtures even by thermal treatment at temperature as high as 1,300–1,350 °C. Mg2SnO4 prepared by annealing the activated mixture has been characterized by diffuse reflectance FT-IR spectroscopy, modulated temperature differential scanning calorimetry, scanning electron microscopy, and specific surface area measurements (B.E.T. method).

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Manuscript Submission: HERE

  • Impact Factor (2019): 2.731
  • Scimago Journal Rank (2019): 0.415
  • SJR Hirsch-Index (2019): 87
  • SJR Quartile Score (2019): Q3 Condensed Matter Physics
  • SJR Quartile Score (2019): Q3 Physical and Theoretical Chemistry
  • Impact Factor (2018): 2.471
  • Scimago Journal Rank (2018): 0.634
  • SJR Hirsch-Index (2018): 78
  • SJR Quartile Score (2018): Q2 Condensed Matter Physics
  • SJR Quartile Score (2018): Q2 Physical and Theoretical Chemistry

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
4
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)