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  • 1 School of Geoscience and Surveying Engineering, China University of Mining & Technology, Beijing 100083, China
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Abstract

The thermal behavior of kaolinite–dimethylsulfoxide intercalation complex was investigated by thermogravimetry (TG) and differential scanning calorimetry (DSC) analysis, X-ray diffraction (XRD) analysis, and Fourier-transform infrared (FT-IR) spectroscopic analysis. The samples gradually heated up to different temperatures were studied by XRD and FT-IR. The kaolinite–dimethylsulfoxide intercalation complex is stable below 130 °C. With the rise in the temperature, the relative intensity of the 1.124-nm peak gradually decreased and disappeared at 200 °C, however, the intensity of the 0.714 nm peak increased in the XRD patterns. In the infrared spectra, the appearance of methyl bands at 3018, 2934, 1428, and 1318 cm−1 indicates the presence of intercalated dimethylsulfoxide, the intensities of these bands decreased with the temperature rising and remained until around 175 °C, which agree with the XRD and TG–DSC data.

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  • SJR Quartile Score (2019): Q3 Condensed Matter Physics
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  • SJR Hirsch-Index (2018): 78
  • SJR Quartile Score (2018): Q2 Condensed Matter Physics
  • SJR Quartile Score (2018): Q2 Physical and Theoretical Chemistry

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
4
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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