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  • 1 Facoltà di Scienze Istituto Dipartimentale di Chimica e Chimica Industriale Italy
  • 2 Facoltà di Ingegneria Università di Catania Viale a. Doria 6 95125 Catania Italy
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The solid-state syntheses of complexes of uranyl acetate dihydrate andN-phenylthiourea have been attempted by heating various stoichiometric mixtures of the reactants directly in a DSC and in a TA apparatus. Both the DSC and the TG results indicate that only the 1∶1 adduct is formed, independently of the molar ratios of the reactants. It appears that the reaction is complete only with a large excess ofN-phenylthiourea, in agreement with IR data.

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