Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 33: Issue 1
Determination of reaction rate parameters using heat conduction microcalorimetry
Authors:
A. Bakri Department of Pharmaceutical Chemistry, Faculty of Pharmacy State University of Utrecht Catharijnesingel 60 3511 Gh Utrecht The Netherlands

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L. H. M. Janssen Department of Pharmaceutical Chemistry, Faculty of Pharmacy State University of Utrecht Catharijnesingel 60 3511 Gh Utrecht The Netherlands

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J. Wilting Department of Pharmaceutical Chemistry, Faculty of Pharmacy State University of Utrecht Catharijnesingel 60 3511 Gh Utrecht The Netherlands

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Pages:
185–190
Online Publication Date:
25 Jul 2005
Publication Date:
01 Mar 1988
Article Category:
Research Article
DOI:
https://doi.org/10.1007/bf01914598
Restricted access

By using the LKB 2277 thermal activity monitor, it is demonstrated that both ampoule and flow-through modes can be used to monitor the reaction parameters for chemical reactions. Theoretical relationships applicable to first-order reactions are proposed and compared with those reported in the literature. Mathematical relationships applicable to second-order reactions are also proposed. The experimental results confirmed the validity of the theoretical relationships and showed that flow microcalorimetry is a rapid technique in kinetic studies.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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