Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 33: Issue 1
Disc — A differential isoperibol scanning calorimeter
Authors:
W. BrillMax-Planck-Institut Für Festkörperforschung Postfach 80 06 65 7000 Stuttgart 80 Germany

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E. GmelinMax-Planck-Institut Für Festkörperforschung Postfach 80 06 65 7000 Stuttgart 80 Germany

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Pages:
365–370
Online Publication Date:
25 Jul 2005
Publication Date:
01 Mar 1988
Article Category:
Research Article
DOI:
https://doi.org/10.1007/bf01914625
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The construction and operation of a new fully automated microcalorimeter is described.This instrument allows specific heat measurements to be performed on small samples in the 10 mg-range at low temperatures (10 K <T < 350 K). The new method consists of ombining the non-adiabatic relaxation-time calorimetry with a twin arrangement and simultaneous temperature scanning. Some experimental details of the calorimeter and sample holders are presented. The accuracy of the calorimeter was verified by calibration measurements on 56 mg of copper. An energy resolution of 0.1μJ/K has been reached near 12 K. To demonstrate the reliability of the microcalorimeter the heat capacity of the new highTc superconductor YBa2Cu3O7−y, was determined.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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