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  • 1 Department of Chemistry Friedrich-Schiller-University A.-Bebel-Str. 2 6900 Jena Germany
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Comparative thermogravimetric and heat-flux DSC investigations of phase formations by heating of sinteractive powders, which were prepared by thermal decomposition of a NiCO3∶ MnCO3=1∶2 mixture and thermal decomposition of oxalate mixed crystals NiMn2(C2O4)3.6H2O, show the metastability of the defect spinel from the oxalate precursor and its high reactivity.

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