Authors:
A. M. Gadalla Chemical Engineering Department Texas A & M University 77843 College Station TX USA

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Hsuan -Fu Yu Chemical Engineering Department Texas A & M University 77843 College Station TX USA

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Fine, hollow, spherical particles with an average size of one micronmeter were formed through pyrolysis of aerosol of nickel nitrate solution. The aerosol product obtained by fast heating to 450°C consisted of tiny crystallites of NiO, hydrated nitrate, and other non-crystalline phase(s). By heating above 480°C, it consisted only of crystalline NiO. To understand the reactions occurring during the aerosolization process, thermal analysis was conducted on nickel nitrate hexahydrate in stagnant and flowing air using different heating rates. The mechanism for the decomposition of nickel(II) nitrate hexahydrate is proposed.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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