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  • 1 Area Ricerca Roma IMAI-CNR C. P. 10 Monterotondo Scalo Roma
  • | 2 Dipart. Chimica Universita La Sapienza Roma Italy
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The Zr, Ti, Sn and Ge hydrogenphosphates, generally prepared in a crystalline form by the refluxing method, have been submitted to hydrothermal treatment at 180° and 300°C in order to observe if the preparation time can be shortened maintaining their chemical composition and their α-structure. Simultaneous TG and DTA together with XRD revealed to be very suitable techniques for the characterization of the obtained products.

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