Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 38: Issue 4
Development of a new equipment for applying the constant rate thermal analysis (CRTA) to temperature programmed oxidation (TPO) of catalysis
Authors:
C. Real Instituto de Ciencias de Materiales Centro Coordinado Universidad de Sevilla-C.S.I.C Apdo. 1115 Sevilla Spain

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M. D. Alcalá Instituto de Ciencias de Materiales Centro Coordinado Universidad de Sevilla-C.S.I.C Apdo. 1115 Sevilla Spain

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J. M. Criado Instituto de Ciencias de Materiales Centro Coordinado Universidad de Sevilla-C.S.I.C Apdo. 1115 Sevilla Spain

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Pages:
797–802
Online Publication Date:
02 Aug 2005
Publication Date:
01 Apr 1992
Article Category:
Research Article
DOI:
https://doi.org/10.1007/bf01979411
Keywords:
constant rate thermal analysis; new equipment; Temperature Programmed Oxidation
Restricted access

A new equipment has been developed in order to apply the constant rate thermal analysis method (CRTA) to Temperature Programmed Oxidation (TPO) processes. The exhausted gases flow through an electrochemical oxygen sensor after leaving the reactor in order to monitor the oxygen consumption in the reaction. The control of the sample temperature is carried out by interfacing both the furnace and the electrical signal of the oxygen sensor to a PID controller that allows to monitor the sample temperature in such a way that the consumption of oxygen is a constant value previously selected by the user.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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