Authors:
E. Gundlach Departments of Chemistry and Materials Science and Engineering, The Ohio State University, 43210-1173 Columbus, OH USA

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P. Gallagher Departments of Chemistry and Materials Science and Engineering, The Ohio State University, 43210-1173 Columbus, OH USA

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Abstract  

The goal of this research is to prepare a series of alloys having sharp, reproducible magnetic transitions for calibrating temperature in thermogravimetry from the magnetic transition temperature of pure cobalt (1121°C) to below room temperature. Alloys in the Ni-Co and Ni-Cu systems were prepared by the thermal decomposition of coprecipitated oxalates in argon. The alloys were subsequently annealed under 5% hydrogen. Magnetic transition temperatures were measured using simultaneous thermomagnetometry/differential thermal analysis. Transition temperatures were corrected using well known meltingpoint standards. Magnetic transition temperatures along with precision are reported as a function of composition.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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