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  • 1 Eidgenössische Technische Hochschule, TCL, CH-8092 Zürich
  • | 2 Mettler-Toledo AG, Analytical, CH-8603 Schwerzenbach, Switzerland
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Abstract  

ADSC with its periodical temperature programs combines the features of DSC measured at high heating rate (high sensitivity) with those at low heating rate (high temperature resolution). In addition, the “reversing” cp effects can be separated from the “non-reversing” latent heat effects. Various periodical temperature programs can be applied. This paper compares the different possible temperature programs and their algorithms for the cp determination for metal, metal oxide and polymer of various properties. Simulated and measured results for various wave shapes and samples are presented. The relevant sample properties and their influence on the measurements are identified and guiding rules for the proper choice of the various experimental parameters are given. Measurements with different samples, performed with the new METTLER TOLEDO STARe-System, are shown and compared with the simulation results. The simulations and the measurements clearly show that the alternating techniques can yield new information about sample properties, but are susceptible to the proper choice of the various experimental parameters.

Manuscript Submission: HERE

  • Impact Factor (2019): 2.731
  • Scimago Journal Rank (2019): 0.415
  • SJR Hirsch-Index (2019): 87
  • SJR Quartile Score (2019): Q3 Condensed Matter Physics
  • SJR Quartile Score (2019): Q3 Physical and Theoretical Chemistry
  • Impact Factor (2018): 2.471
  • Scimago Journal Rank (2018): 0.634
  • SJR Hirsch-Index (2018): 78
  • SJR Quartile Score (2018): Q2 Condensed Matter Physics
  • SJR Quartile Score (2018): Q2 Physical and Theoretical Chemistry

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
4
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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