A new micro reaction calorimeter

R. Hart; J. Jones

doi:10.1007/bf01996800

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Journal of Thermal Analysis and Calorimetry

Volume/Issue:: Volume 49: Issue 2

A new micro reaction calorimeter

Authors:

R. Hart

R. Hart Hart R and D Inc., 84647 Mt. Pleasant, Ut USA

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and

J. Jones

J. Jones Astra Scientific International Inc., 6900 Koll Center Parkway Suite #417, 94566 Pleasanton, CA USA

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Pages:: 1115–1119

Online Publication Date:: 05 Aug 2005

Publication Date:: 01 Aug 1997

Article Category:: Research Article

DOI:: https://doi.org/10.1007/bf01996800

Keywords:: hazards; microcalorimeter; physiology; portable; safety; titration

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Abstract

Traditional reaction calorimeters require highly trained operators and the use of a large sample size (10 ml to 1000 ml) which is incompatible with highly reactive substances. A new calorimeter with a 2 ml or less sample size lends itself to the determination of reactivity of materials for process safety and to the determination of safety of materials shipped in compartment tank cars. The TC-100 Titration Calorimeter meets these requirements. A cost effective instrumentation of a differential cell design provides high sensitivity heat flow measurements. Automatic liquid injection and continuous mixing provides information on the heat of reaction and its rate. A portable instrument with small sample size allows for rapid temperature equilibration and safe handling of very reactive materials.

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Journal of Thermal Analysis and Calorimetry

Print ISSN:: 1388-6150

Online ISSN:: 1572-8943

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Journal of Thermal Analysis and Calorimetry
Language	English
Size	A4
Year of Foundation	1969
Volumes per Year	1
Issues per Year	24
Founder	Akadémiai Kiadó
Founder's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher	Akadémiai Kiadó Springer Nature Switzerland AG
Publisher's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible Publisher	Chief Executive Officer, Akadémiai Kiadó
ISSN	1388-6150 (Print)
ISSN	1588-2926 (Online)