Author:
P. S. Bassi Chemistry Department, Guru Nanak Dev University, 143006 Amritsar, India

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Abstract

TG-DTG-DTA has been used to characterize various isomers of CoCl2·2(CH3C6H4NH2). Thermal analysis is further used to analyse the binary mixtures of these isomers. DTA recorded after different elapsed times follows the progress of reaction between cobalt chloride and benzocaine where progressively small endotherms are associated with starting materials. The application of thermal analysis to following the solid-solid reactions between metal acetates and 8-hydroxyquinoline was highlighted. The stoichiometry of such reactions was confirmed from the decrease in intensity of an endotherm as one increases the stoichiometry.

  • 1 Kambe, H. Garn, D. D. 1974 Thermal Analysis John Wiley and Sons New York.

  • 2 Brown, W. E. Dollimore, D. Galwey, A. K. 1980 Comprehensive Chemical Kinetics, Vol. 22 Elsevier Amsterdam.

  • 3 Bassi, P. S. Randhawa, B. S. Jamwal, H. S. 1983 Thermochem. Acta 71 1515. .

  • 4 Bassi, P. S. Randhawa, B. S. Jamwal, H. S. 1985 Thermochim. Acta 86 141141. .

  • 5 Bassi, P. S. Randhawa, B. S. Khajuria, C. M. Kaur, Sandeep 1987 J. Thermal Anal. 32 569569. .

  • 6 Bassi, P. S. Chopra, G. S. Kaur, K. 1989 J. Thermal Anal. 35 12131213. .

  • 7 Bassi, P. S. Chopra, G. S. Kaur, K. 1990 Indian J. Chem. 29A 454454.

  • 8 Bassi, P. S. Randhawa, B. S. Kaur, Sandeep 1992 Indian J. Chem. 31A 596596.

  • 9 Bassi, P. S. Chopra, G. S. Singh, Rajinder 1996 Indian J. Chem. 35A 458458.

  • 10 Vogel's Textbook of Practical Organic Chemistry, 5th Edition, Longman 1989, p. 701.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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