Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 50: Issue 5-6
About the thermal decomposition of tetracyanocomplexes
Authors:
J. Bubanec Department of Inorganic Chemistry, Faculty of Sciences, P. J. Safarik's University, 04154 Kosice, Slovak Republic

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A. Sopková Department of Inorganic Chemistry, Faculty of Sciences, P. J. Safarik's University, 04154 Kosice, Slovak Republic

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Pages:
831–841
Online Publication Date:
02 Aug 2005
Publication Date:
01 Dec 1997
Article Category:
Research Article
DOI:
https://doi.org/10.1007/bf01979213
Keywords:
electron microscopy; inclusion compounds; thermal decomposition products; topochemical reactions
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Abstract  

Tetracyanocomplex clathrates and their changes caused by heating were studied. The intermediates formed were characterized by IR and UV-VIS spectroscopy. Elemental analysis and XRD patterns were also used. For the visualisation of changes occurring on the surface and the distribution of metallic elements therein were studied by electron microscopy and EDX. The extent of the non-stoichiometric changes introduced by the topochemical course of the degradation reactions was correlated with the measured electrical values.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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