Authors:
J. Bubanec Department of Inorganic Chemistry, Faculty of Sciences, P. J. Safarik's University, 04154 Kosice, Slovak Republic

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A. Sopková Department of Inorganic Chemistry, Faculty of Sciences, P. J. Safarik's University, 04154 Kosice, Slovak Republic

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Abstract  

Tetracyanocomplex clathrates and their changes caused by heating were studied. The intermediates formed were characterized by IR and UV-VIS spectroscopy. Elemental analysis and XRD patterns were also used. For the visualisation of changes occurring on the surface and the distribution of metallic elements therein were studied by electron microscopy and EDX. The extent of the non-stoichiometric changes introduced by the topochemical course of the degradation reactions was correlated with the measured electrical values.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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