Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 53: Issue 1
Vapour Pressure and Thermoanalytical Study of Diethyldithiocarbamates of Platinum Metals
Authors:
S. Sysoev Institute of Inorganic Chemistry Novosibirsk Russian Novosibirsk Russian

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N. Morozova Institute of Inorganic Chemistry Novosibirsk Russian Novosibirsk Russian

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G. Zharkova Institute of Inorganic Chemistry Novosibirsk Russian Novosibirsk Russian

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I. Igumenov Institute of Inorganic Chemistry Novosibirsk Russian Novosibirsk Russian

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P. Semyannikov Institute of Inorganic Chemistry Novosibirsk Russian Novosibirsk Russian

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V. Grankin Institute of Inorganic Chemistry Novosibirsk Russian Novosibirsk Russian

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Pages:
87–96
Online Publication Date:
03 Nov 2004
Publication Date:
01 May 1998
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1010157907718
Keywords:
diethyldithiocarbamates of platinum metals; DTA; vapour pressure
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Abstract  

A thermoanalytical study of the diethyldithiocarbamates of the platinum metals Pt(II), Pd(II), Rh(III), Ir(III) and Ru(III) was carried out by means of DTA techniques in an inert atmosphere and in vacuum. Decomposition temperatures were determined and the mass loss curves were obtained for these compounds in helium and in vacuum. The X-ray diffraction patterns of the solid products of M(dtk)n thermolysis were studied. The temperature dependences of the saturated vapour pressures of the listed chelates were measured by flow and Knudsen methods, and the vaporization parameters were determined.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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