Authors:
J. Kristóf University of Veszprém Department of Analytical Chemistry H-8201 Veszprém PO Box 158 Hungary H-8201 Veszprém PO Box 158 Hungary

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R. Frost Queensland University of Technology Centre for Instrumental and Developmental Chemistry 2 George Street GPO Box 2434 Brisbane Queensland 4001 Australia 2 George Street GPO Box 2434 Brisbane Queensland 4001 Australia

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E. Horváth Hungarian Academy of Sciences Research Group for Analytical Chemistry H-8201 Veszprém PO Box 158 Hungary H-8201 Veszprém PO Box 158 Hungary

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L. Kocsis Hungarian Academy of Sciences Research Group for Analytical Chemistry H-8201 Veszprém PO Box 158 Hungary H-8201 Veszprém PO Box 158 Hungary

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J. Inczédy University of Veszprém Department of Analytical Chemistry H-8201 Veszprém PO Box 158 Hungary H-8201 Veszprém PO Box 158 Hungary

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Abstract  

The thermal behaviour of ordered kaolinites from Hungary and Australia intercalated with potassium acetate, cesium acetate and urea has been investigated by simultaneous TG-DTG-DTA, TG-MS, Raman microscopy and XRD. Remarkable changes in the thermal decomposition pattern of the intercalates were obtained as a function of the nature of the intercalating re-agents. Replacing the potassium cation to cesium leads to a change in the OH environments resulting in a more complicated dehydroxylation pattern. The urea intercalates can be decomposed completely without dehydroxylating the mineral, although further treatments are necessary to restore the original d-spacing.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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