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R. Denoyel Centre du Thermodynamique et de Microcalorimétrie du CNRS 26 rue du 141 13331 Marseille France 26 rue du 141 13331 Marseille France

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M. Keene Centre du Thermodynamique et de Microcalorimétrie du CNRS 26 rue du 141 13331 Marseille France 26 rue du 141 13331 Marseille France

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P. Llewellyn Centre du Thermodynamique et de Microcalorimétrie du CNRS 26 rue du 141 13331 Marseille France 26 rue du 141 13331 Marseille France

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J. Rouquerol Centre du Thermodynamique et de Microcalorimétrie du CNRS 26 rue du 141 13331 Marseille France 26 rue du 141 13331 Marseille France

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Abstract  

The synthesis of new ordered mesoporous adsorbents, specifically of the MCM-41 type, involves a step of thermal elimination of the template (a surfactant) where CRTA is shown to provide a 'soft chemistry' route. Once the mesoporous (i.e. 2 to 50 nm pore width) material is obtained, the pore size is determined by thermoporometry, a convenient application for low temperature DSC. Finally, the hydrophobic - hydrophilic properties of the pore walls are explored by immersion microcalorimetry in water.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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