Authors:
A. Béres József Attila University Applied Chemistry Department Rerrich B. tér 1 Szeged Rerrich B. tér 1 Szeged

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I. Pálinkó József Attila University Department of Organic Chemistry Dóm tér 8 Szeged H-6720 Hungary Dóm tér 8 Szeged H-6720 Hungary

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Á. Fudala József Attila University Applied Chemistry Department Rerrich B. tér 1 Szeged Rerrich B. tér 1 Szeged

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I. Kiricsi József Attila University Applied Chemistry Department Rerrich B. tér 1 Szeged Rerrich B. tér 1 Szeged

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Y. Kiyozumi National Institute of Materials and Chemical Research Molecular Recognition Laboratory 1-1 Higashi, Tsukuba Ibaraki Japan 1-1 Higashi, Tsukuba Ibaraki Japan

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F. Mizukami National Institute of Materials and Chemical Research Molecular Recognition Laboratory 1-1 Higashi, Tsukuba Ibaraki Japan 1-1 Higashi, Tsukuba Ibaraki Japan

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J. Nagy Universitaires Notre-Dame de la Paix Unité de RMN, Facultés 61 rue Bruxelles Namur B-5000 Belgique 61 rue Bruxelles Namur B-5000 Belgique

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Abstract  

Mg-Al L(ayered) D(ouble) H(ydroxide) was prepared and its thermal behaviour was characterized by thermoanalytical methods (TG, DTG, DTA), 27Al M(agic) A(ngle) S(pinning) NMR spectroscopy, X-ray diffractometry (XRD) and S(canning) E(lectron) M(icroscopy). Heat treatment destroyed the layered structure, which could only be partially reconstituted by rehydration. On calcination mixed oxide with the predominance of basic sites were formed. Pillaring the LDH with Fe(CN)64- anions was also performed. The material was characterized by XRD and BET measurements. Heat stability of the pillared substance was investigated, too. Pillaring proved to be successful, however, decreased heat resistance was found in the intercalated material relative to the guest LDH.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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