Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 56: Issue 1
Behaviour of Hydrotalcite and Its Fe (CN)64- Pillared Derivative on Heat Treatment
Authors:
A. Béres József Attila University Applied Chemistry Department Rerrich B. tér 1 Szeged Rerrich B. tér 1 Szeged

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I. Pálinkó József Attila University Department of Organic Chemistry Dóm tér 8 Szeged H-6720 Hungary Dóm tér 8 Szeged H-6720 Hungary

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Á. Fudala József Attila University Applied Chemistry Department Rerrich B. tér 1 Szeged Rerrich B. tér 1 Szeged

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I. Kiricsi József Attila University Applied Chemistry Department Rerrich B. tér 1 Szeged Rerrich B. tér 1 Szeged

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Y. Kiyozumi National Institute of Materials and Chemical Research Molecular Recognition Laboratory 1-1 Higashi, Tsukuba Ibaraki Japan 1-1 Higashi, Tsukuba Ibaraki Japan

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F. Mizukami National Institute of Materials and Chemical Research Molecular Recognition Laboratory 1-1 Higashi, Tsukuba Ibaraki Japan 1-1 Higashi, Tsukuba Ibaraki Japan

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J. Nagy Universitaires Notre-Dame de la Paix Unité de RMN, Facultés 61 rue Bruxelles Namur B-5000 Belgique 61 rue Bruxelles Namur B-5000 Belgique

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Pages:
311–316
Online Publication Date:
03 Nov 2004
Publication Date:
01 Jul 1999
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1010138314956
Keywords:
dehydration/rehydration and stability characterization; Fe(CN)64- anion pillared layered double hydroxide; Mg-Al layered double hydroxide; thermal behaviour
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Abstract  

Mg-Al L(ayered) D(ouble) H(ydroxide) was prepared and its thermal behaviour was characterized by thermoanalytical methods (TG, DTG, DTA), 27Al M(agic) A(ngle) S(pinning) NMR spectroscopy, X-ray diffractometry (XRD) and S(canning) E(lectron) M(icroscopy). Heat treatment destroyed the layered structure, which could only be partially reconstituted by rehydration. On calcination mixed oxide with the predominance of basic sites were formed. Pillaring the LDH with Fe(CN)64- anions was also performed. The material was characterized by XRD and BET measurements. Heat stability of the pillared substance was investigated, too. Pillaring proved to be successful, however, decreased heat resistance was found in the intercalated material relative to the guest LDH.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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