Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 56: Issue 2
Thermal Behaviour and Analytical Study of the Production of TiSnOx from the Mixed 8-Hydroxyquinolinates
Authors:
L. Guinesi Instituto de Química-UNESP R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil

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M. Crespi Instituto de Química-UNESP R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil

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C. Ribeiro Instituto de Química-UNESP R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil

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J. Nagata Instituto de Química-UNESP R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil R. Prof. Francisco Degni, s/n C.P. 355 Araraquara-SP Brazil

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Pages:
525–531
Online Publication Date:
08 Dec 2004
Publication Date:
01 Sep 1999
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1010152627465
Keywords:
ceramic precursor; thermogravimetry; TiSnOx
Restricted access

Abstract  

Solubility and pH precipitation studies were carried out to obtain the binuclear complex {[TiO(C9H6NO)2][Sn(C9H6NO)2]} involving 8-hydroxyquinoline as chelating agent. The compound, the individual mononuclear complexes and their physical mixture were evaluated by means of techniques such as TG, DTA, elemental analysis, X-ray diffraction, IR spectroscopy. The properties of the original compounds and also the thermoanalytical conditions exerted a great influence on the degree of crystallinity and on the crystalline phase of the mixed oxide obtained as final product of the thermal decomposition.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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