Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 56: Issue 3
Modulated Differential Scanning Calorimetry Analysis of Interphases in Multi-Component Polymer Materials
Authors:
M. Song Loughborough University IPTME Loughborough LE11 3TU Loughborough LE11 3TU

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D. Hourston Loughborough University IPTME Loughborough LE11 3TU Loughborough LE11 3TU

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M. Reading Loughborough University IPTME Loughborough LE11 3TU Loughborough LE11 3TU

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H. Pollock Lancaster University School of Physics and Chemistry UK UK

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A. Hammiche Lancaster University School of Physics and Chemistry UK UK

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Pages:
991–1004
Online Publication Date:
16 Aug 2006
Publication Date:
01 Nov 1999
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1010167920138
Keywords:
interfaces; interpenetrating polymer networks; latex; M-TDSC; polymer blends
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Abstract  

A modulated-temperature differential scanning calorimetry (M-TDSC) method for the analysis of interphases in multi-component polymer materials has been developed further. As examples, interphases in a polybutadiene-natural rubber (50:50 by mass) blend, a poly(methyl methacrylate)-poly(vinyl acetate) (50:50 by mass) structured latex film, a polyepichlorohydrinpoly(vinyl acetate) bilayer film, and polystyrene-polyurethane (40:60 by mass) and poly(ethyl methacrylate)-polyurethane (60:40 by mass) interpenetrating polymer networks were investigated. The mass fraction of interphase and its composition can be calculated quantitatively. These interphases do not exhibit clear separate glass transition temperatures, but occur continually between the glass transition temperatures of the constituent polymers.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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