Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 58: Issue 2
Decomposition of Cyclohexyl-t-butyl-Dimethylammonium Tetraphenylborate: Synthesis and kinetics
Authors:
B. Zhou Harbin Institute of Technology Department of Natural Science Weihai Campus Weihai, Shandong Province 264209 P. R. China Weihai Campus Weihai, Shandong Province 264209 P. R. China

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S. Jiang Harbin Institute of Technology Department of Natural Science Weihai Campus Weihai, Shandong Province 264209 P. R. China Weihai Campus Weihai, Shandong Province 264209 P. R. China

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L. Zou Shandong Yantai Teacher's College Department of Chemistry Yantai, Shandong Province 264025 P. R. China Yantai, Shandong Province 264025 P. R. China

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X. Wang Shandong Yantai Teacher's College Department of Chemistry Yantai, Shandong Province 264025 P. R. China Yantai, Shandong Province 264025 P. R. China

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D. Wang Shandong Normal University Department of Chemistry Jinan, Shandong Province 250014 P. R. China Jinan, Shandong Province 250014 P. R. China

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J. Liu Shandong Normal University Department of Chemistry Jinan, Shandong Province 250014 P. R. China Jinan, Shandong Province 250014 P. R. China

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S. Shang Shandong Normal University Department of Chemistry Jinan, Shandong Province 250014 P. R. China Jinan, Shandong Province 250014 P. R. China

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D. Zhou Harbin Institute of Technology Department of Natural Science Weihai Campus Weihai, Shandong Province 264209 P. R. China Weihai Campus Weihai, Shandong Province 264209 P. R. China

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Pages:
487–493
Online Publication Date:
25 Oct 2004
Publication Date:
25 Nov 1999
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1010184028318
Keywords:
non-isothermal kinetics; quaternary ammonium; tetraphenylborate; thermal decomposition
Restricted access

Abstract  

A new compound cyclohexyl-t-butyldimethylammonium tetraphenylborate, [C6H11N(CH3)2(C(CH3)3)]BPh4 has been prepared, and its decomposition mechanism was studied by TG. The IR spectra of the products of thermal decomposition were examined at every stage. Kinetic analysis for the first stage of thermal decomposition process was obtained by TG and DTG curves, and kinetic parameters were obtained from the analysis of the TG-DTG curves with integral and differential equations. The most probable kinetic function was suggested by comparison of kinetic parameters.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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