Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 59: Issue 3
Synthesis, Characterization and Thermal Studies of Some Iron(III) Complexes of o-Vanillin Oxime
Authors:
M. Kurup Cochin University of Science and Technology Department of Applied Chemistry Kochi 682 022 India Kochi 682 022 India

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E. Lukose St. Joseph's College for Women Department of Chemistry Alappuzha 688 001 India Alappuzha 688 001 India

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K. Muraleedharan Cochin University of Science and Technology Department of Applied Chemistry Kochi 682 022 India Kochi 682 022 India

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Pages:
815–825
Online Publication Date:
02 Nov 2004
Publication Date:
01 Mar 2000
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1010109905765
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Abstract  

Iron(III) complexes of o-vanillin oxime have been synthesized and characterized by different physicochemical techniques. The complexes containing thiocyanate, iodide and sulphate ionshave been subjected to non-isothermal decomposition studies in N2 using TGand DTG techniques. The kinetic parameters for both stages of decomposition of these complexes were evaluated by weighted least-squares method using the general approach as well as the Coats–Redfern and Horowitz–Metzger equations. The results indicate that the values of kinetic parameters obtained by these three different approaches agree well.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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