Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 62: Issue 1
Method of Separating the Sensitive Volume of Calorimetric Cells in a Differential Titration Calorimeter
Authors:
G. Kotelnikov Russian Academy of Sciences Institute for Biological Instrumentation 142292 Pushchino Moscow Region Russia 142292 Pushchino Moscow Region Russia

Search for other papers by G. Kotelnikov in
Current site
Google Scholar
PubMed Close
,
S. Moiseyeva Russian Academy of Sciences Institute for Biological Instrumentation 142292 Pushchino Moscow Region Russia 142292 Pushchino Moscow Region Russia

Search for other papers by S. Moiseyeva in
Current site
Google Scholar
PubMed Close
,
E. Mezhburd Russian Academy of Sciences Institute for Biological Instrumentation 142292 Pushchino Moscow Region Russia 142292 Pushchino Moscow Region Russia

Search for other papers by E. Mezhburd in
Current site
Google Scholar
PubMed Close
, and
V. Krayev Russian Academy of Sciences Institute for Biological Instrumentation 142292 Pushchino Moscow Region Russia 142292 Pushchino Moscow Region Russia

Search for other papers by V. Krayev in
Current site
Google Scholar
PubMed Close
Pages:
39–50
Online Publication Date:
02 Nov 2004
Publication Date:
01 Oct 2000
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1010150409126
Keywords:
differential titration calorimeter; heat-conducting bridge; sensitive volumes of calorimetric cells
Restricted access

Abstract  

A scientific and technical solution of capillary calorimetric unit design is described based on a method of separating the sensitive volume of calorimetric cells with a heat-conducting bridge in a differential titration calorimeter. The design of the calorimetric cells as thin capillary tubes allowed to minimize the dimension of the heat-conducting bridges and to separate with high accuracy the sensitive volume of the calorimetric cells which is of 78.5 μl. Due to high calorimeter power sensitivity (10 nW) a modern level of requirements for measuring minimum specific heat of processes is provided. The adopted design of the calorimetric cells permits to possess the cells located horizontally and to simplify the solution of the problem of equalizing components concentration along the volume of the calorimetric cells.

  • Collapse
  • Expand
Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

To see the editorial board, please visit the website of Springer Nature.

Manuscript Submission: HERE

For subscription options, please visit the website of Springer Nature.

Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

Monthly Content Usage

Abstract Views Full Text Views PDF Downloads
Apr 2024 6 0 0
May 2024 0 0 0
Jun 2024 2 0 0
Jul 2024 1 0 0
Aug 2024 7 0 0
Sep 2024 10 0 0
Oct 2024 0 0 0