Authors:
J. Mano Universidade do Minho Departamento de Engenharia de Polímeros Campus de Azurém 4800-058 Guimarães Portugal Campus de Azurém 4800-058 Guimarães Portugal

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S. Lanceros-Méndez Universidade do Minho Departamento de Física Campus de Gualtar 4710 Braga Codex Portugal Campus de Gualtar 4710 Braga Codex Portugal

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A. Nunes Universidade Nova de Lisboa Departamento de Química, Centro de Química Fina e Biotecnologia, Faculdade de Cięncias e Tecnologia 2825-114 Monte de Caparica Portugal 2825-114 Monte de Caparica Portugal

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M. Dionísio Universidade Nova de Lisboa Departamento de Química, Centro de Química Fina e Biotecnologia, Faculdade de Cięncias e Tecnologia 2825-114 Monte de Caparica Portugal 2825-114 Monte de Caparica Portugal

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Abstract  

Dielectric experiments are often performed in non-isothermal conditions. Thus, there is a difference between the temperature of the sample and the sensor temperature. In this work we propose and compare three temperature calibration methods based on the detection of transitions or relaxations: i) the melting of high-purity metallic standards (indium and tin), ii) the 2nd order phase transition of a ferroelectric crystal (TGS); iii) the -relaxation of an amorphous polymer (poly(carbonate)). The results obtained from the three different methods were used to construct a calibration curve for a given heating rate.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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