Authors:
L. Wang Chinese Academy of Sciences Thermochemistry Laboratory, Dalian Institute of Chemical Physics Dalian 116023 China Dalian 116023 China

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Z. Tan Chinese Academy of Sciences Thermochemistry Laboratory, Dalian Institute of Chemical Physics Dalian 116023 China Dalian 116023 China

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S. Meng Chinese Academy of Sciences Thermochemistry Laboratory, Dalian Institute of Chemical Physics Dalian 116023 China Dalian 116023 China

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D. Liang Chinese Academy of Sciences Environmental Engineering Laboratory, Dalian Institute of Chemical Physics Dalian 116023 China Dalian 116023 China

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S. Ji Dalian Maritime University Institute of Material and Technology Dalian 116026 China Dalian 116026 China

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Z. Hei Dalian Maritime University Institute of Material and Technology Dalian 116026 China Dalian 116026 China

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Abstract  

Fe–B ultrafine amorphous alloy particles (UFAAP) were prepared by chemical reduction of Fe3+ with NaBHO4 and confirmed to be ultrafine amorphous particles by transmission electron microscopy and X-ray diffraction. The specific heat of the sample was measured by a high precision adiabatic calorimeter, and a differential scanning calorimeter was used for thermal stability analysis. A topological structure of Fe-B atoms is proposed to explain two crystallization peaks and a melting peak observed at T=600, 868 and 1645 K, respectively.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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