Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 66: Issue 3
Thermal Analysis, EPR and XPS Study of Vanadyl(IV) Oxalate Behavior on the Ceria Surface
Authors:
J. Matta Université du Littoral – Côte d'Opale, MREID Laboratoire de Catalyse et Environnement – E.A.2598 145, avenue Maurice Schumann F-59140 Dunkerque France 145, avenue Maurice Schumann F-59140 Dunkerque France

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D. Courcot Université du Littoral – Côte d'Opale, MREID Laboratoire de Catalyse et Environnement – E.A.2598 145, avenue Maurice Schumann F-59140 Dunkerque France 145, avenue Maurice Schumann F-59140 Dunkerque France

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E. Abi-Aad Université du Littoral – Côte d'Opale, MREID Laboratoire de Catalyse et Environnement – E.A.2598 145, avenue Maurice Schumann F-59140 Dunkerque France 145, avenue Maurice Schumann F-59140 Dunkerque France

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A. Aboukaïs Université du Littoral – Côte d'Opale, MREID Laboratoire de Catalyse et Environnement – E.A.2598 145, avenue Maurice Schumann F-59140 Dunkerque France 145, avenue Maurice Schumann F-59140 Dunkerque France

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Pages:
717–727
Online Publication Date:
26 Oct 2004
Publication Date:
01 Dec 2001
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1013131819569
Keywords:
cerium oxalates; EPR; thermal analysis; vanadium oxalates; XPS
Restricted access

Abstract  

The thermal decomposition of vanadyl oxalatesupported on CeO2 solid in a flow of dried air was analysed by thermogravimetry (TG) and differential scanning calorimetry (DSC) from room temperature up to 350C. TG and DSC results have demonstrated that after the impregnation of CeO2 solid by a vanadyl oxalate solution, cerium and vanadium(V) oxalates were evidenced. This latter compound seems attached to cerium(III) of the partial reduced CeO2 phase. This result was confirmed with the electron paramagnetic resonance(EPR) and X-ray photoelectron spectroscopy (XPS) techniques.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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