Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 66: Issue 3
Thermal Analysis in Structural Characterization of Hydrazone Ligands and Their Complexes
Authors:
K. Andjelković University of Belgrade Faculty of Chemistry Studentski trg. 16 P.O. Box 158 YU-11001 Belgrade Yugoslavia

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M. Šumar University of Belgrade Faculty of Chemistry Studentski trg. 16 P.O. Box 158 YU-11001 Belgrade Yugoslavia

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I. Ivanović-Burmazović University of Belgrade Faculty of Chemistry Studentski trg. 16 P.O. Box 158 YU-11001 Belgrade Yugoslavia

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Pages:
759–778
Online Publication Date:
26 Oct 2004
Publication Date:
01 Dec 2001
Article Category:
Research Article
DOI:
https://doi.org/10.1023/a:1013140021386
Keywords:
hydrazone ligands; thermal analysis; transition metal complexes
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Abstract  

Results of our research on synthesis and characterization of complexes with acylhydrazone derivatives are described in this review paper. Structural characterization of newly synthesized complexes by thermal analysis (TG, DTA, DSC) is particularly emphasized in this paper. Thermal analysis enabled us to study not only structural changes of substances during thermal treatment, but also the mode of coordination and degree of deprotonation of acylhydrazones, as well as geometry of the coordination sphere of complexes, the structure of which had not been determined by X-ray analysis. Topics in this paper are as follows: complexes of dioxomolybdenum(VI) with tridentate hydrazones, usnic acid derivatives and their Cu(II) complexes, as well as transition metal complexes with 2,6-diacetylpyridine bis(hydrazones).

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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