Authors:
Á. GombÁs University of Szeged Department of Pharmaceutical Technology H-6720 Szeged Eötvös u. 6 Hungary H-6720 Szeged Eötvös u. 6 Hungary

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P. Szabó-Révész University of Szeged Department of Pharmaceutical Technology H-6720 Szeged Eötvös u. 6 Hungary H-6720 Szeged Eötvös u. 6 Hungary

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M. Kata University of Szeged Department of Pharmaceutical Technology H-6720 Szeged Eötvös u. 6 Hungary H-6720 Szeged Eötvös u. 6 Hungary

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G. Regdon University of Szeged Department of Pharmaceutical Technology H-6720 Szeged Eötvös u. 6 Hungary H-6720 Szeged Eötvös u. 6 Hungary

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I. Erős University of Szeged Department of Pharmaceutical Technology H-6720 Szeged Eötvös u. 6 Hungary H-6720 Szeged Eötvös u. 6 Hungary

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Abstract  

In pharmaceutical practice it is important and useful to know the crystallinity of materials and to monitor it during formulation development, production processes and storage. The purpose of this study was to assess the quantitative capability of DSC for determining crystallinity in crystalline/amorphous powder mixtures and to compare the accuracy of the DSC method with that of conventional powder X-ray diffraction. Alpha-lactose monohydrate was chosen as the model material. On the basis of this study it can be concluded, that DSC method can be applied safely for semiquantitative evaluation of the crystallinity of lactose samples consisting of an amorphous content higher than 20%.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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