Authors:
R. Campostrini Universita di Trento Dipartimento di Ingegneria dei materiali via Mesiano 77 38050 Trento Italy via Mesiano 77 38050 Trento Italy

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M. Ischia Universita di Trento Dipartimento di Ingegneria dei materiali via Mesiano 77 38050 Trento Italy via Mesiano 77 38050 Trento Italy

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L. Palmisano Universita di Palermo Dipartimento di Ingegneria Chimica dei Processi e dei Materiali Viale delle Scienze 90128 Palermo Italy Viale delle Scienze 90128 Palermo Italy

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Abstract  

A homogeneous TiO2 gel was obtained by hydrolysing titanium(IV) isopropoxide that was previously modified by reaction with acetic acid. The so stabilized precursor was hydrolysed under strong acidic medium (pH=0 by HCl). Dried TiO2 powders were characterized by FT-IR, XRD, N2 adsorption analyses, coupled thermogravimetric (TG) gas chromatographic (GC) and `mass spectrometric (MS) analyses. A semiquantitative analysis of the main evolved chemical species allowed to depict both the chemical rearrangements occurring in the TiO2 matrix during pyrolysis and the chemical composition of the initial gel.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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