Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 75: Issue 1
Pyrolysis study of sol—gel derived TiO2 powders: Part III. TiO2-anatase prepared by reacting titanium(IV) isopropoxide with acetic acid
Authors:
R. Campostrini Universita di Trento Dipartimento di Ingegneria dei materiali via Mesiano 77 38050 Trento Italy via Mesiano 77 38050 Trento Italy

Search for other papers by R. Campostrini in
Current site
Google Scholar
PubMed Close
,
M. Ischia Universita di Trento Dipartimento di Ingegneria dei materiali via Mesiano 77 38050 Trento Italy via Mesiano 77 38050 Trento Italy

Search for other papers by M. Ischia in
Current site
Google Scholar
PubMed Close
, and
L. Palmisano Universita di Palermo Dipartimento di Ingegneria Chimica dei Processi e dei Materiali Viale delle Scienze 90128 Palermo Italy Viale delle Scienze 90128 Palermo Italy

Search for other papers by L. Palmisano in
Current site
Google Scholar
PubMed Close
Pages:
13–24
Online Publication Date:
02 Nov 2004
Publication Date:
25 Jan 2004
Article Category:
Research Article
DOI:
https://doi.org/10.1023/b:jtan.0000017324.05515.b9
Keywords:
thermogravimetric-mass spectrometric coupled analyses; pyrolysis study; TiO2 gel
Restricted access

Abstract  

A homogeneous TiO2 gel was obtained by hydrolysing titanium(IV) isopropoxide that was previously modified by reaction with acetic acid. The so stabilized precursor was hydrolysed under strong acidic medium (pH=0 by HCl). Dried TiO2 powders were characterized by FT-IR, XRD, N2 adsorption analyses, coupled thermogravimetric (TG) gas chromatographic (GC) and `mass spectrometric (MS) analyses. A semiquantitative analysis of the main evolved chemical species allowed to depict both the chemical rearrangements occurring in the TiO2 matrix during pyrolysis and the chemical composition of the initial gel.

  • Collapse
  • Expand
Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

To see the editorial board, please visit the website of Springer Nature.

Manuscript Submission: HERE

For subscription options, please visit the website of Springer Nature.

Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

Monthly Content Usage

Abstract Views Full Text Views PDF Downloads
Nov 2024 13 0 0
Dec 2024 6 0 0
Jan 2025 7 0 0
Feb 2025 14 0 0
Mar 2025 15 0 0
Apr 2025 8 0 0
May 2025 1 0 0