Authors:
L. Machado Universidade Federal do Espírito Santo Departamento de Química 29060-900 Vitória - ES Brazil E-mail 29060-900 Vitória - ES Brazil E-mail

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A. Marins Universidade Federal do Espírito Santo Departamento de Química 29060-900 Vitória - ES Brazil E-mail 29060-900 Vitória - ES Brazil E-mail

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E. Muri Universidade Federal do Espírito Santo Departamento de Química 29060-900 Vitória - ES Brazil E-mail 29060-900 Vitória - ES Brazil E-mail

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J. Lacerda Universidade Federal do Espírito Santo Departamento de Química 29060-900 Vitória - ES Brazil E-mail 29060-900 Vitória - ES Brazil E-mail

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V. Balthar Universidade Federal do Espírito Santo Departamento de Química 29060-900 Vitória - ES Brazil E-mail 29060-900 Vitória - ES Brazil E-mail

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P. Fulvio Universidade Federal do Espírito Santo Departamento de Química 29060-900 Vitória - ES Brazil E-mail 29060-900 Vitória - ES Brazil E-mail

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J. Freitas Universidade Federal do Espírito Santo Departamento de Física 29060-900 Vitória - ES Brazil 29060-900 Vitória - ES Brazil

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Abstract  

This paper presents the reactions of synthesis between the ligand sodium diphenylamine-4-sulfonate and the lanthanum(III) chloride hydrated. The compounds (LaCl3)2(C12H10NSO3Na)32(CH3CH2OH) (A) and (LaCl3)(C12H10NSO3Na)(CH3CH2OH)12H2O (B) were obtained using the solvents ethanol and methanol (synthesis A) and ethanol and water (synthesis B). The produced compounds and the ligand were characterized by thermogravimetric and differential thermogravimetric analysis, IR spectroscopy and elemental analysis of sodium, carbon, hydrogen, nitrogen, sulfur, chlorine and lanthanum, whereas the residues from thermal decomposition were investigated by X-ray diffractometry.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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