Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 78: Issue 2
The coupled TG-MS investigations of lanthanide(III) nitrate complexes with hexamethylenetetramine
Authors:
M. Zalewicz University of Technology Institute of General and Ecological Chemistry, Łódź Żekomskiego 116 90-924 Łódź Poland Żekomskiego 116 90-924 Łódź Poland

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and
A. Trzesowska University of Technology Institute of General and Ecological Chemistry, Łódź Żekomskiego 116 90-924 Łódź Poland Żekomskiego 116 90-924 Łódź Poland

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Pages:
525–534
Online Publication Date:
07 Dec 2004
Publication Date:
01 Nov 2004
Article Category:
Research Article
DOI:
https://doi.org/10.1023/b:jtan.0000046116.43443.36
Keywords:
thermogravimetry; lanthanide complexes; mass spectroscopy; hexamethylenetetramine
Restricted access

Abstract  

New transition metal compounds of the general formula Ln(NO3)32[N4(CH2)6]nH2O, where Ln = La, Nd, Sm, Gd, Tb, Dy, Er, Lu, and n = 7-12, were obtained. The compounds and the gases evolved in the course of their thermal decomposition were characterised by thermogravimetric analysis. The measurements were carried out in air and argon environment in order to compare the intermediate products, final products and the mechanism of the thermal decomposition. The combined TG-MS system was used to identify the main volatile products of thermal decomposition and fragmentation processes of the obtained compounds.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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