Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 81: Issue 3
Water adsorption and desorption on microporous solids at elevated temperature
Authors:
M. S. Gruszkiewicz Chemical Sciences Division, Aqueous Chemistry and Geochemistry Group, Oak Ridge National Laboratory Oak Ridge, Tennessee 37831, USA

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J. M. Simonson Chemical Sciences Division, Aqueous Chemistry and Geochemistry Group, Oak Ridge National Laboratory Oak Ridge, Tennessee 37831, USA

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T. D. Burchell Metals and Ceramics Division, Oak Ridge National Laboratory Oak Ridge, Tennessee 37831, USA

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D. R. Cole Chemical Sciences Division, Aqueous Chemistry and Geochemistry Group, Oak Ridge National Laboratory Oak Ridge, Tennessee 37831, USA

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Pages:
609–615
Online Publication Date:
08 Sep 2005
Publication Date:
01 Aug 2005
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-005-0832-1
Keywords:
adsorption; water; zeolite; carbon fiber; gravimetric; high-temperature; pillared clay; porous glass
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Summary An accurate gravimetric method was used to explore water adsorption/desorption isotherms between 105 and to 250°C for a number of synthetic and natural porous solids including controlled pore glass, activated carbon fiber monoliths, natural zeolites, pillared clay, and geothermal reservoir rocks.  The main goal of this work was to evaluate water adsorption results, in particular temperature dependence of hysteresis, for relatively uniform, nano-structured solids, in the context of other state-of-the-art experimental and modeling methods including nitrogen adsorption, spectroscopy, neutron scattering, and molecular simulation. Since no single method is able to provide a complete characterization of porous materials, a combination of approaches is needed to achieve progress in understanding the fluid-solid interactions on the way to developing a predictive capability.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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