Authors:
H. Yu Analysis and Testing Center for Inorganic Materials, Shanghai Institute of Ceramics, Chinese Academy of Sciences 1295 Dingxi Rd., 200050 Shanghai, P. R. China 1295 Dingxi Rd., 200050 Shanghai, P. R. China

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C. Lu Analysis and Testing Center for Inorganic Materials, Shanghai Institute of Ceramics, Chinese Academy of Sciences 1295 Dingxi Rd., 200050 Shanghai, P. R. China 1295 Dingxi Rd., 200050 Shanghai, P. R. China

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T. Xi Analysis and Testing Center for Inorganic Materials, Shanghai Institute of Ceramics, Chinese Academy of Sciences 1295 Dingxi Rd., 200050 Shanghai, P. R. China 1295 Dingxi Rd., 200050 Shanghai, P. R. China

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L. Luo Analysis and Testing Center for Inorganic Materials, Shanghai Institute of Ceramics, Chinese Academy of Sciences 1295 Dingxi Rd., 200050 Shanghai, P. R. China 1295 Dingxi Rd., 200050 Shanghai, P. R. China

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J. Ning The State Key Laboratory of High Performance Ceramics and Superfine Structure, Shanghai Institute of Ceramics, Chinese Academy of Sciences 1295 Dingxi Rd., 200050 Shanghai, P. R. China 1295 Dingxi Rd., 200050 Shanghai, P. R. China

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C. Xiang The State Key Laboratory of High Performance Ceramics and Superfine Structure, Shanghai Institute of Ceramics, Chinese Academy of Sciences 1295 Dingxi Rd., 200050 Shanghai, P. R. China 1295 Dingxi Rd., 200050 Shanghai, P. R. China

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Summary  

TG-DSC-MS (thermogravimetry-differential scanning calorimetry-mass spectrometry) coupling techniques were used to make a simultaneous characterizing study for the thermal decomposition process of the carbon nanotube (CNT)/SiO2precursor powders prepared by rapid sol-gel method. The thermal stability of the CNT and the SiO2pure gel were investigated by TG-DSC. The results showed that the oxidation of CNT began from 530 and combusted at about 678C at the heating rate of 10C min-1in air. Moreover, the faster the heating rate, the higher the temperature of CNT combustion. The appropriate calcinations temperature of the CNT/SiO2precursor powders should be held for 1 h at 500C.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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