Authors: Q Kwok 1 and R Seyler 2
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  • 1 Canadian Explosives Research Laboratory Ottawa Canada K1A 0G1 ON Ottawa Canada K1A 0G1 ON
  • | 2 Tredegar Film Products Terre Haute USA 47804 IN Terre Haute USA 47804 IN
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Abstract  

ASTM Committee E37 on Thermal Measurements published a new test method 'Standard Test Method for Volatility Rate by Thermogravimetry' in June 1999 with the designation E 2008. This approach to assessing volatility utilizes an extension of the pinhole technology previously employed by E37 for vapor pressure determinations using differential scanning calorimetry (ASTM E 1782). After publication of the test method E 2008, an Interlaboratory Study was undertaken to develop a 'Precision and Bias' statement to be assigned with the test method. This paper provides some background data that supports the claim that E 2008 is generally insensitive to experimental conditions other than temperature. The Interlaboratory Study showing the statistical review is also discussed.

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