Authors:
M. Alonso Universidad Complutense de Madrid Departamento de Ingeniería Química, Facultad de Ciencias Químicas Madrid Spain 28040 Madrid Spain 28040

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M. Oliet Universidad Complutense de Madrid Departamento de Ingeniería Química, Facultad de Ciencias Químicas Madrid Spain 28040 Madrid Spain 28040

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J. García Universidad Complutense de Madrid Departamento de Ingeniería Química, Facultad de Ciencias Químicas Madrid Spain 28040 Madrid Spain 28040

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F. Rodríguez Universidad Complutense de Madrid Departamento de Ingeniería Química, Facultad de Ciencias Químicas Madrid Spain 28040 Madrid Spain 28040

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J. Echeverría Hexion Ibérica, Carretera a Navarra Hernani, Guipúzcoa Spain 20120 Epele 39 Hernani, Guipúzcoa Spain 20120 Epele 39

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Abstract  

Kinetics of thermosetting polymers curing is difficult to study by isothermal methods based on the differential scanning calorimetry (DSC) technique. The difficulty is due to the low sensitivity of the equipment for total reaction heat measurements during high temperature process. The aim of this paper is to display the equivalence between a dynamic model, the Ozawa method, and an isothermal isoconversional fit, which allows predicting the isothermal behavior of the resol resins cure through dynamic runs by DSC. In this work, lignin–phenol–formaldehyde and commercial phenol–formaldehyde resol resins were employed. In addition, the isothermal kinetic parameters for both resins were performed by means of transformation of the data obtained from the dynamic Ozawa method.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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