Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 87: Issue 3
Influence of processing conditions on the thermal decomposition of SrTiO3 precursors
Authors:
Márcia Silva Universidade Federal da Paraíba LTM, Departamento de Química/CCEN João Pessoa Brazil CEP 58059-900 PB Campus I João Pessoa Brazil CEP 58059-900 PB Campus I

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L. Soledade Universidade Federal da Paraíba LTM, Departamento de Química/CCEN João Pessoa Brazil CEP 58059-900 PB Campus I João Pessoa Brazil CEP 58059-900 PB Campus I

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S. Lima UFPB Laboratório de Solidificação Rápida/CT João Pessoa Brazil PB João Pessoa Brazil PB

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E. Longo UNESP CDMC/LIEC/Instituto de Química Araraquara Brazil SP Araraquara Brazil SP

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A. Souza Universidade Federal da Paraíba LTM, Departamento de Química/CCEN João Pessoa Brazil CEP 58059-900 PB Campus I João Pessoa Brazil CEP 58059-900 PB Campus I

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Iêda Santos Universidade Federal da Paraíba LTM, Departamento de Química/CCEN João Pessoa Brazil CEP 58059-900 PB Campus I João Pessoa Brazil CEP 58059-900 PB Campus I

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Pages:
731–735
Online Publication Date:
09 Mar 2007
Publication Date:
01 Mar 2007
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-006-7766-0
Keywords:
atmosphere; milling; Pechini method; SrTiO3; thermal decomposition
Restricted access

Abstract  

The present work investigates the influence of milling and calcination atmosphere on the thermal decomposition of SrTiO3 powder precursors. Both pure and neodymium-modified SrTiO3 samples were studied. Milling did not significantly influence numerical mass loss value, but reduced the number of decomposition steps, modifying the profiles of the TG and DTA curves. On the other hand, milling increases the amount of energy liberated by the system upon combustion of organic matter. It was also observed that the milling process, associated to the calcination in an oxygen atmosphere, considerably decreases the amount of organic matter and increases the final mass loss temperature.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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