Authors:
N. Turta Al. I. Cuza, University of Iasi Faculty of Chemistry, Department of Physical Chemistry, Theoretical and Materials Chemistry Iasi Romania 700506 11 Carol I Bd.

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D. Vuono University of Calabria Department of Pianificazione Territoriale Arcavacata di Rende (CS) Italy 87036 via P. Bucci

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P. De Luca University of Calabria Department of Pianificazione Territoriale Arcavacata di Rende (CS) Italy 87036 via P. Bucci

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N. Bilba Al. I. Cuza, University of Iasi Faculty of Chemistry, Department of Physical Chemistry, Theoretical and Materials Chemistry Iasi Romania 700506 11 Carol I Bd.

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A. Nastro University of Calabria Department of Pianificazione Territoriale Arcavacata di Rende (CS) Italy 87036 via P. Bucci

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Abstract  

The aim of this paper is to define the characteristics of crystalline phase ETS-10 obtained from gel with dodecyltrimethylammonium bromide, as an organic template. ETS-10 zeolites has been synthesised under hydrothermal conditions from gels of composition 5Na2O–3KF–TiO2–6.4HCl– xC12TMAB –7.45SiO2–197.5H2O (where x=0.0, 0.25, 0.55, 1.0 and 1.5) with dodecyltrimethylammonium bromide. The crystalline phases synthesised with organic salt have an exothermal peak at ca. 360°C, due to the degradation of organic entrapped in the porous structure. Physical-chemical properties of C12TMAB -ETS-10 are studied by XRD, SEM and thermal analyses.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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