Authors:
Anna Kropidłowska Gdańsk University of Technology Inorganic Chemistry Department Gdańsk Poland 80-952 Narutowicza Str. 11/12 Gdańsk Poland 80-952 Narutowicza Str. 11/12

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M. Strankowski Gdańsk University of Technology Polymer Technology Department, Chemical Faculty Gdańsk Poland 80-952 Narutowicza Str. 11/12 Gdańsk Poland 80-952 Narutowicza Str. 11/12

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Maria Gazda Gdańsk University of Technology Faculty of Applied Physics and Mathematics Gdańsk Poland 80-952 Narutowicza Str. 11/12 Gdańsk Poland 80-952 Narutowicza Str. 11/12

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Barbara Becker Gdańsk University of Technology Inorganic Chemistry Department Gdańsk Poland 80-952 Narutowicza Str. 11/12 Gdańsk Poland 80-952 Narutowicza Str. 11/12

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Abstract  

The thermal behavior of Mn(II) silanethiolate series [Mn(SR)2L(MeOH)n], where R=SSi(OBut)3, L=heterocyclic nitrogen base and n=0, 1 or 2 has been comparatively investigated using differential scanning calorimetry (DSC), thermogravimetry (TG) and TG-infrared spectoscopy (IR) techniques. The TG curves indicate the differences in the thermal decomposition due to presence of distinct N-donor ligands and labile MeOH molecules coordinated to the central atom. The first step on the TG curves (60–110C) corresponds to the elimination of alcohol from respective complexes. The main step (150–350C) can be assigned to the decomposition of the complexes yielding Mn3O4 and silica as the main final products, identified by X-ray diffraction patterns.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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