Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 90: Issue 2
Temperature programmed desorption analysis of sol-gel-derived titania films
Design of a sol preparation procedure
Authors:
T. Nishide Nihon University Department of Materials Chemistry and Engineering, College of Engineering Tamura, Koriyama 963-8642 Japan

Search for other papers by T. Nishide in
Current site
Google Scholar
PubMed Close
,
T. Tanaka Nihon University Department of Materials Chemistry and Engineering, College of Engineering Tamura, Koriyama 963-8642 Japan

Search for other papers by T. Tanaka in
Current site
Google Scholar
PubMed Close
, and
T. Yabe Nihon University Department of Materials Chemistry and Engineering, College of Engineering Tamura, Koriyama 963-8642 Japan

Search for other papers by T. Yabe in
Current site
Google Scholar
PubMed Close
Pages:
373–378
Online Publication Date:
11 Jul 2007
Publication Date:
01 Nov 2007
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-007-7791-7
Keywords:
anatase; photocatalysis; temperature programmed desorption; thin film; titania
Restricted access

Abstract  

Sol-gel-derived titania films were analyzed by temperature programmed desorption (TPD) and X-ray diffraction (XRD) techniques. The relationship between the TPD curves measured for two types of titania gel films and their crystal structures was investigated. On the basis of the analyses, a preparation process for a titania sol solution containing anatase nanocrystals was designed and developed. Using this process, a colloidal anatase titania sol solution was prepared by heating aqueous titanium hydroxide containing HCl at 60�C for 2 h. The nanocrystal structure of the titania films obtained by coating the sol on glass substrates was confirmed by TPD and XRD measurements.

  • Collapse
  • Expand
Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

To see the editorial board, please visit the website of Springer Nature.

Manuscript Submission: HERE

For subscription options, please visit the website of Springer Nature.

Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

Monthly Content Usage

Abstract Views Full Text Views PDF Downloads
Aug 2024 5 0 0
Sep 2024 17 0 0
Oct 2024 66 0 0
Nov 2024 9 0 0
Dec 2024 3 0 0
Jan 2025 5 0 0
Feb 2025 2 0 0