Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 90: Issue 2
Structural and thermal characterization of Fe(III) and Fe(II) complexes with tridentate ONO pyridoxal semicarbazone
Authors:
Ž. Jaćimović University of Montenegro Faculty of Metallurgy and Technology Podgorica Montenegro

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V. Leovac University of Novi Sad Faculty of Sciences, Department of Chemistry Novi Sad Serbia

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G. Giester Universität Wien Institut für Mineralogie und Kristallographie Wien Austria

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Z. Tomić Laboratory of Theoretical Physics and Condensed Matter Physics Vinča’ Institute of Nuclear Sciences P.O. Box 522 11001 Belgrade Serbia

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Katalin Szécsényi University of Novi Sad Faculty of Sciences, Department of Chemistry Novi Sad Serbia

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Pages:
549–555
Online Publication Date:
07 Dec 2007
Publication Date:
01 Nov 2007
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-006-8267-x
Keywords:
crystal structure; deaquation mechanism; iron(II) and iron(III) complexes; pyridoxal semicarbazone thermal decomposition
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Abstract  

Molecular and crystal structure of diaqua-sulphato(pyridoxal semicarbazone-ONO)iron(II) and dichloroaqua(pyridoxal semicarbazone-ONO)iron(III) complexes with tridentate ONO pyridoxal semicarbazone ligand, PLSC, of formula [FeII(PLSC)(H2O)2SO4] and [FeIII(PLSC)(H2O)Cl2]Cl is reported. Thermal decomposition of the compounds was followed in argon and air gas carriers. The dequation mechanism is discussed in the view of the crystal structure, emphasizing the complexity of the related parameters and processes.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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