Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 92: Issue 3
Crystal solvates of tetrakis(3,5-di- t -butylphenyl)-porphyrinates Mn(III), Ni(II) and Zn(II) with pyridine
Authors:
E. Balantseva Ivanovo State University of Chemistry and Technology F. Engels av. 7 153000 Ivanovo Russia

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E. Antina Russian Academy of Sciences Institute of Solution Chemistry Akademicheskaya Street, 1 153045 Ivanovo Russia

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M. Berezin Russian Academy of Sciences Institute of Solution Chemistry Akademicheskaya Street, 1 153045 Ivanovo Russia

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A. Vyugin Russian Academy of Sciences Institute of Solution Chemistry Akademicheskaya Street, 1 153045 Ivanovo Russia

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Pages:
671–675
Online Publication Date:
02 Jul 2008
Publication Date:
01 Jun 2008
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-008-9012-4
Keywords:
axial coordination; crystal solvate; molecular complexes; tetrakis(3,5-di-t-butylphenyl)porphin; TG
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Abstract  

The crystal solvates of complexes MP (P is the dianion of tetrakis(3,5-di-t-butylphenyl)porphin, M=Ni(II), Zn(II)) and (Ac)MnP with pyridine have been obtained by isothermal evaporation of corresponding solutions at 35°C. The formation and the decomposition temperatures of crystal solvates and enthalpies of evaporation pyridine molecules from those crystal solvates were received using thermogravimetric method. In addition to that, an influence of the type of metal on the compositions, the energetic and thermal stabilities of the received complexes were analyzed.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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