Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 92: Issue 3
Study of thermal behavior of α-PbO2, using TG and DSC
Authors:
S. Sajadi Sharif University of Technology Institute of Water & Energy P.O.Box 11365-8639 Tehran Iran

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A. Alamolhoda Sharif University of Technology Institute of Water & Energy P.O.Box 11365-8639 Tehran Iran

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, and
S. Hashemian Sharif University of Technology Institute of Water & Energy P.O.Box 11365-8639 Tehran Iran

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Pages:
917–920
Online Publication Date:
02 Jul 2008
Publication Date:
01 Jun 2008
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-007-8687-2
Keywords:
DSC; lead(IV) oxide; TG; thermal analysis; XRD
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Abstract  

Using two techniques of thermogravimetry and differential scanning calorimetry under O2 gas atmosphere from 25 to 600°C, the thermal behavior of laboratory-produced compound lead(IV) oxide α-PbO2 was investigated. The identity of products at different stages were confirmed by XRD technique. Both techniques produced similar results supporting the same decomposition stages for the compound. Three distinct energy changes were observed, namely, two endothermic and one exothermic in DSC. The amount of ΔH for each peak is also reported.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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