Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 92: Issue 3
Synthesis, characterization and thermal behaviour of solid 2-methoxybenzoates of trivalent metals
Authors:
A. Siqueira Instituto de Química UNESP, CP 355 CEP 14801-970 Araraquara, SP Brazil

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C. Carvalho Instituto de Química UNESP, CP 355 CEP 14801-970 Araraquara, SP Brazil

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E. Ionashiro Universidade Estadual de Ponta Grossa CEP 84010-919 Ponta Grossa, PR Brazil

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G. Bannach Universidade Estadual de Ponta Grossa CEP 84010-919 Ponta Grossa, PR Brazil

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E. Rodrigues Fundação Educacional de Barretos CEP 14780-000 Barretos, SP Brazil

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M. Ionashiro Instituto de Química UNESP, CP 355 CEP 14801-970 Araraquara, SP Brazil

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Pages:
945–951
Online Publication Date:
02 Jul 2008
Publication Date:
01 Jun 2008
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-007-8546-1
Keywords:
characterization; heavier lanthanides; 2-methoxybenzoate; thermal behaviour
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Abstract  

Solid-state Ln(L)3 compounds, where Ln stands for trivalent Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu and Y and L is 2-methoxybenzoate have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results provided information on the composition, dehydration, coordination mode, structure, thermal behaviour and thermal decomposition.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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