Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 92: Issue 3
2-Methoxybenzylidenepyruvatewith heavier trivalent lanthanides and yttrium(III)
Synthesis and characterization
Authors:
E. Ionashiro Instituto de Química UNESP, C.P. 355 CEP 14801-970 Araraquara, SP Brasil

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G. Bannach Instituto de Química UNESP, C.P. 355 CEP 14801-970 Araraquara, SP Brasil

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A. Siqueira Instituto de Química UNESP, C.P. 355 CEP 14801-970 Araraquara, SP Brasil

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C. de Carvalho Instituto de Química UNESP, C.P. 355 CEP 14801-970 Araraquara, SP Brasil

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E. Rodrigues Fundação Educacional de Barretos CEP 14780-000 Barretos, SP Brazil

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M. Ionashiro Instituto de Química UNESP, C.P. 355 CEP 14801-970 Araraquara, SP Brasil

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Pages:
953–959
Online Publication Date:
02 Jul 2008
Publication Date:
01 Jun 2008
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-007-8699-y
Keywords:
characterization; heavier lanthanides; yttrium; 2-methoxybenzylidenepyruvate; thermal behaviour
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Abstract  

Solid-state Ln(2-MeO-BP) compounds, where Ln stands for trivalent Eu to Lu and Y(III) and 2-MeO-BP (which is 2-methoxybenzylidenepyruvate) have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffraction, infrared spectroscopy and other methods of analysis were used to characterize and to study these compounds. On the base of the obtained results an Ln(2MeO-BP)3·nH2O general formula can be established.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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