Authors:
Lucia Odochian’Al. I. Cuza’ University, Faculty of Chemistry 11 Carol I Bd Iassy Romania

Search for other papers by Lucia Odochian in
Current site
Google Scholar
PubMed
Close
,
Anca Mocanu’Gh. Asachi’ University, Faculty of Chemical Engineering 71A D. Mangeron Bd Iassy Romania

Search for other papers by Anca Mocanu in
Current site
Google Scholar
PubMed
Close
,
C. Moldoveanu’Al. I. Cuza’ University, Faculty of Chemistry 11 Carol I Bd Iassy Romania

Search for other papers by C. Moldoveanu in
Current site
Google Scholar
PubMed
Close
,
Gabriela Carja’Gh. Asachi’ University, Faculty of Chemical Engineering 71A D. Mangeron Bd Iassy Romania

Search for other papers by Gabriela Carja in
Current site
Google Scholar
PubMed
Close
, and
C. Oniscu’Gh. Asachi’ University, Faculty of Chemical Engineering 71A D. Mangeron Bd Iassy Romania

Search for other papers by C. Oniscu in
Current site
Google Scholar
PubMed
Close
Restricted access

Abstract  

The paper deals with the characterization of three hydrazinic complexes with Ni, Cu and Cr respectively, by means of non-isothermal thermal methods, TG, DTG and DTA, under nitrogen atmosphere in order to investigate the structure-thermostability-thermal degradation mechanism correlation. The thermal analysis made evident the degradation mechanisms characteristic of every sample in accordance with the chemical structure. The quantitative analysis by TG-DTG afforded the estimation of the metal amount in the complex on the basis of the resulting metallic oxide nature as well as of some aspects of the thermal degradation mechanism supported by mass spectral measurements. The melting points given by DTA and confirmed by the Boetius method and the initial temperatures of thermal degradation from TG-DTG-DTA afforded to ascertain the temperature range proper for using and storing the complexes under study which show potential practical applications as drugs.

  • Collapse
  • Expand

To see the editorial board, please visit the website of Springer Nature.

Manuscript Submission: HERE

For subscription options, please visit the website of Springer Nature.

Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

Monthly Content Usage

Abstract Views Full Text Views PDF Downloads
Aug 2022 0 0 0
Sep 2022 1 0 0
Oct 2022 2 0 0
Nov 2022 0 0 0
Dec 2022 1 0 1
Jan 2023 0 0 0
Feb 2023 0 0 0