Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 95: Issue 2
Preparation and characterization of nano-ZnO flakes prepared by reactive ion exchange method
Authors:
Y. Li Dalian Jiaotong University College of Environmental and Chemical Engineering Dalian 116028 China

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G. Li Dalian Jiaotong University College of Environmental and Chemical Engineering Dalian 116028 China

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,
S. Wang Dalian Jiaotong University College of Environmental and Chemical Engineering Dalian 116028 China

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H. Gao Dalian Jiaotong University College of Environmental and Chemical Engineering Dalian 116028 China

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, and
Z. Tan

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Pages:
671–674
Online Publication Date:
15 Aug 2008
Publication Date:
01 Feb 2009
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-008-9042-y
Keywords:
adiabatic calorimetry; heat capacity; nano-ZnO flakes; reactive ion exchange synthesis
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Abstract  

Nano-ZnO flakes were synthesized by calcination of the precursor of Zn(OH)2 obtained via the reactive ion exchange method between an ion exchange resin and ZnSO4 solution at room temperature. Scanning electron microscopy, X-ray diffraction, energy dispersive X-ray spectroscope, UV-Vis diffuse reflection spectrum and Na2EDTA titration were used to characterize the structure features and chemical compositions of the as-prepared ZnO. The results show that the as-prepared ZnO flakes have uniform structure and high purity. Heat capacities in the temperature range of 83 to 396 K were measured. The measured heat capacities values were compared with those of coarse crystal powders and the difference between this two heat capacity curves was analyzed.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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